Information card for entry 7105092

Structure parameters

• Formula: C31 H26 Cl2 Co2 O11
• Calculated formula: C31 H26 Cl2 Co2 O11
• Title of publication: Preparation of highly substituted tetrahydropyrans via a metal assisted dipolar cycloaddition reaction
• Authors of publication: Eric A. Allart; Steven D. R. Christie; Gareth J. Pritchard; Mark R. J. Elsegood
• Journal of publication: Chem. Commun.
• Year of publication: 2009
• Pages of publication: 7339 - 7341
• a: 9.2516 ± 0.0012 Å
• b: 13.8248 ± 0.0019 Å
• c: 14.022 ± 0.0019 Å
• α: 109.652 ± 0.0019°
• β: 91.9541 ± 0.0019°
• γ: 104.885 ± 0.0019°
• Cell volume: 1617.9 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1044
• Residual factor for significantly intense reflections: 0.0774
• Weighted residual factors for significantly intense reflections: 0.216
• Weighted residual factors for all reflections included in the refinement: 0.2425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No