Information card for entry 7105243

Structure parameters

• Formula: C75 H57 N12 O11 Te7
• Calculated formula: C75 H57 N12 O11 Te7
• Title of publication: Hydrolysis of 2-phenylazophenyltellurium trihalides: isolation of an unprecedented homometallic, discrete heptanuclear organotellurium oxide cluster.
• Authors of publication: Srivastava, Kriti; Sharma, Sagar; Singh, Harkesh B; Singh, Udai P; Butcher, Ray J
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 7
• Pages of publication: 1130 - 1132
• a: 11.5886 ± 0.0002 Å
• b: 15.0996 ± 0.0002 Å
• c: 21.7891 ± 0.0004 Å
• α: 86.278 ± 0.001°
• β: 87.151 ± 0.001°
• γ: 77.097 ± 0.001°
• Cell volume: 3706.19 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0609
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0832
• Weighted residual factors for all reflections included in the refinement: 0.0881
• Goodness-of-fit parameter for all reflections included in the refinement: 0.972
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No