Information card for entry 7105329

Structure parameters

• Formula: C57 H48 P4 Se6 Te
• Calculated formula: C57 H48 P4 Se6 Te
• Title of publication: Novel carbon-centred reactivity of [(H)C(PPh2Se)2]- in the formation of structurally diverse Sn(IV), Te(IV) and Hg(II) complexes of the triseleno ligand [(Se)C(PPh2Se)2]2-.
• Authors of publication: Konu, Jari; Chivers, Tristram
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 9
• Pages of publication: 1431 - 1433
• a: 13.002 ± 0.003 Å
• b: 17.066 ± 0.003 Å
• c: 24.9 ± 0.005 Å
• α: 79.57 ± 0.03°
• β: 87.46 ± 0.03°
• γ: 85.93 ± 0.03°
• Cell volume: 5416.9 ± 1.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0761
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1012
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No