Information card for entry 7105630

Structure parameters

• Formula: C88 H108 Li2 N4 O2 Si2 Y2
• Calculated formula: C88 H108 Li2 N4 O2 Si2 Y2
• Title of publication: Well-defined and easily accessible yttrium complexes for enantioselective cyclisation of amines tethered to 1,2-di-substituted alkenes
• Authors of publication: Chapurina, Yulia; Hannedouche, Jérôme; Collin, Jacqueline; Guillot, Régis; Schulz, Emmanuelle; Trifonov, Alexander
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 37
• Pages of publication: 6918 - 6920
• a: 11.1174 ± 0.0005 Å
• b: 25.9601 ± 0.0012 Å
• c: 27.1473 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7835 ± 0.6 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.0997
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No