Information card for entry 7105649

Structure parameters

• Formula: C9 H10 N O4 Rh S2
• Calculated formula: C9 H10 N O4 Rh S2
• Title of publication: In situ formation of ligand 2,2'-[(E)-diazene-1,2-diyldicarbonothioyl]diphenol and structural characterization of its binuclear rhodium(V) complex containing RhO2+.
• Authors of publication: Gangopadhyay, Snigdha; Basak, Prodyut; Drew, Michael; Gangopadhyay, Pijush Kanti
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 39
• Pages of publication: 7436 - 7438
• a: 7.2911 ± 0.0006 Å
• b: 8.933 ± 0.0008 Å
• c: 10.6189 ± 0.0009 Å
• α: 68.437 ± 0.008°
• β: 87.346 ± 0.007°
• γ: 71.086 ± 0.008°
• Cell volume: 606.4 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0773
• Residual factor for significantly intense reflections: 0.0659
• Weighted residual factors for significantly intense reflections: 0.1844
• Weighted residual factors for all reflections included in the refinement: 0.1909
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No