Information card for entry 7105964

Structure parameters

• Common name: Dichloro-palladium-complex
• Chemical name: Dichloro-palladium-complex
• Formula: C37 H49 Cl6 N O3 P2 Pd Si
• Calculated formula: C37 H49 Cl6 N O3 P2 Pd Si
• Title of publication: Immobilized Sonogashira Catalyst Systems: New Insights by Multinuclear HRMAS NMR Studies
• Authors of publication: Tobias Posset; Johannes Guenther; Jacqueline Pope; Thomas Oeser; Janet Blumel
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 2059
• a: 11.2996 ± 0.0007 Å
• b: 13.4269 ± 0.0008 Å
• c: 28.789 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4367.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.037
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0781
• Weighted residual factors for all reflections included in the refinement: 0.0792
• Goodness-of-fit parameter for all reflections included in the refinement: 1.126
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No