Crystallography Open Database

Information card for entry 7106104

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Coordinates	7106104.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C241 H334 N14 O16 Yb4
Calculated formula	C241 H326 N14 O16 Yb4
Title of publication	The First Bridged Lanthanide Carbene Complex Formed through Reduction of Carbodiimide by amine Bis(phenolate )Ytterbium(II) Complex and Its Reactivity to Phenylisocyanate
Authors of publication	Zhu Du; Hui Zhou; Haisheng Yao; Yong Zhang; Yingming Yao; Qi Shen
Journal of publication	Chem.Commun.
Year of publication	2011
Journal volume	47
Pages of publication	3595
a	57.606 ± 0.004 Å
b	16.958 ± 0.001 Å
c	24.9846 ± 0.0018 Å
α	90°
β	109.757 ± 0.002°
γ	90°
Cell volume	22970 ± 3 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1164
Residual factor for significantly intense reflections	0.0866
Weighted residual factors for significantly intense reflections	0.1751
Weighted residual factors for all reflections included in the refinement	0.1896
Goodness-of-fit parameter for all reflections included in the refinement	1.126
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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