Information card for entry 7106621

Structure parameters

• Formula: C18 H36 Fe Ge2 O
• Calculated formula: C18 H36 Fe Ge2 O
• Title of publication: Trans-selective hydrogermylation of alkynes promoted by methyliron and bis(germyl)hydridoiron complexes as a catalyst precursor
• Authors of publication: Masumi Itazaki; Masahiro Kamitani; Hiroshi Nakazawa
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 7854
• a: 10.44 ± 0.0012 Å
• b: 14.1 ± 0.0014 Å
• c: 16.5 ± 0.0014 Å
• α: 63.3 ± 0.005°
• β: 81.67 ± 0.007°
• γ: 89.18 ± 0.008°
• Cell volume: 2143.4 ± 0.4 ų
• Cell temperature: 190 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.054
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1009
• Weighted residual factors for all reflections included in the refinement: 0.1059
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No