Information card for entry 7109504

Structure parameters

• Formula: C52 H83 Cu7 Dy2 N10 O52.5
• Calculated formula: C26 H27 Cu3.5 Dy N5 O22
• Title of publication: Two 3d-4f nanomagnets formed via a two-step in situ reaction of picolinaldehyde
• Authors of publication: Jun-Liang Liu; Yan-Cong Chen; Quan-Wen Li; Silvia Gomez-Coca; Daniel Aravena; Eliseo Ruiz; Wei-Quan Lin; Ji-Dong Leng; Ming-Liang Tong
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 6549
• a: 11.6017 ± 0.001 Å
• b: 12.0819 ± 0.0009 Å
• c: 15.5313 ± 0.0011 Å
• α: 99.682 ± 0.002°
• β: 102.582 ± 0.002°
• γ: 105.718 ± 0.003°
• Cell volume: 1984.6 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1724
• Residual factor for significantly intense reflections: 0.1141
• Weighted residual factors for significantly intense reflections: 0.2386
• Weighted residual factors for all reflections included in the refinement: 0.2636
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No