Information card for entry 7110316

Structure parameters

• Common name: 03049
• Formula: C46.5 H42 O2 P2 Pd
• Calculated formula: C46.5 H42 O2 P2 Pd
• Title of publication: Mixed metal bis(�-oxo) complexes with [CuM(�-O)2]n+ (M = Ni(iii) or Pd(ii)) coresElectronic supplementary information (ESI) available: experimental and calculation details. See http://www.rsc.org/suppdata/cc/b4/b404640d/
• Authors of publication: Aboelella, Nermeen W.; York, John T.; Reynolds, Anne M.; Fujita, Koyu; Kinsinger, Christopher R.; Cramer, Christopher J.; Riordan, Charles G.; Tolman, William B.
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 15
• Pages of publication: 1716 - 1717
• a: 9.2639 ± 0.0014 Å
• b: 23.168 ± 0.004 Å
• c: 18.26 ± 0.003 Å
• α: 90°
• β: 92.962 ± 0.003°
• γ: 90°
• Cell volume: 3913.8 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0626
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0831
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No