Information card for entry 7110397

Structure parameters

• Formula: C66 H99 N O12 P2 Pt Si8
• Calculated formula: C66 H99 N O12 P2 Pt Si8
• Title of publication: Synthesis and structural characterisation of platinum silasesquioxane complexes
• Authors of publication: Abbenhuis, Hendrikus C. L.; van Santen, Rutger A.; Burrows, Andrew D.; Palmer, Mark T.; Kooijman, Huub; Lutz, Martin; Spek, Anthony L.
• Journal of publication: Chemical Communications
• Year of publication: 1998
• Journal issue: 23
• Pages of publication: 2627
• a: 47.997 ± 0.004 Å
• b: 13.9845 ± 0.0011 Å
• c: 21.803 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14634 ± 2 ų
• Cell temperature: 153 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 7
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.1172
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1071
• Weighted residual factors for all reflections included in the refinement: 0.1439
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No