Information card for entry 7110449

Structure parameters

• Formula: C47 H48 Al B F15 N2 O1.5 Si2
• Calculated formula: C47 H48 Al B F15 N2 O1.5 Si2
• Title of publication: Synthesis and structures of neutral and cationic β-diketiminatoaluminium methyls†
• Authors of publication: Coslédan, Frédéric; Hitchcock, Peter B.; Lappert, Michael F.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 8
• Pages of publication: 705
• a: 12.016 ± 0.003 Å
• b: 13.439 ± 0.005 Å
• c: 16.409 ± 0.007 Å
• α: 99.44 ± 0.03°
• β: 91.8 ± 0.03°
• γ: 108.31 ± 0.02°
• Cell volume: 2471.8 ± 1.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0942
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for all reflections: 0.2013
• Weighted residual factors for significantly intense reflections: 0.1458
• Goodness-of-fit parameter for all reflections: 0.833
• Goodness-of-fit parameter for significantly intense reflections: 0.748
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No