Information card for entry 7110508

Structure parameters

• Formula: H736 Mo154 Na21 O830 P7
• Calculated formula: Mo154 Na4 O752 P7
• Title of publication: Assembling nanosized ring-shaped synthons to an anionic layer structure based on the synergetically induced functional complementarity of their surface-sites: Na21[MoVI126MoV28O462H14(H2O)54(H2PO2)7]·xH2O (x ≈ 300)
• Authors of publication: Müller, Achim; Das, Samar K.; Bögge, Hartmut; Beugholt, Christian; Schmidtmann, Marc
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 11
• Pages of publication: 1035
• a: 50.075 ± 0.003 Å
• b: 56.049 ± 0.004 Å
• c: 30.302 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 85047 ± 10 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 5
• Space group number: 64
• Hermann-Mauguin space group symbol: C m c a
• Hall space group symbol: -C 2ac 2
• Residual factor for all reflections: 0.1625
• Residual factor for significantly intense reflections: 0.0735
• Weighted residual factors for significantly intense reflections: 0.1783
• Weighted residual factors for all reflections included in the refinement: 0.2743
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No