Information card for entry 7110549

Structure parameters

• Formula: C36 H84 Ag7 O12 P6 Se12.5
• Calculated formula: C36 Ag6.994 O12 P6 Se12.497
• Title of publication: Metal dialkyl diselenophosphates:1 a rare example of co-crystallization with clusters, Ag8(μ8-Se)[Se2P(OPri)2]6 and Ag6[Se2P(OPri)2]6, superimposing in a trigonal lattice†
• Authors of publication: Liu, C. W.; Shang, Iu-Jie; Wang, Ju-Chung; Keng, Tai-Chiun
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 11
• Pages of publication: 995
• a: 22.7866 ± 0.0012 Å
• b: 22.7866 ± 0.0012 Å
• c: 12.8738 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5788.9 ± 0.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0446
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for all reflections: 0.0992
• Weighted residual factors for all reflections included in the refinement: 0.0943
• Goodness-of-fit parameter for all reflections: 1.069
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No