Information card for entry 7110565

Structure parameters

• Formula: C20 H134 Mo6 N10 O106 S8 Si2 W22
• Calculated formula: C14 Mo6 N7 O110 S8 Si2 W22
• Title of publication: ‘Adding’ stable functional complementary, nucleophilic and electrophilic clusters: a synthetic route to [{(SiW11O39)Mo3S4(H2O)3(μ-OH)}2]10− and [{(P2W17O61)Mo3S4(H2O)3(μ-OH)}2]14− as examples
• Authors of publication: Müller, Achim; Fedin, Vladimir P.; Kuhlmann, Christoph; Bögge, Hartmut; Hauptfleisch, Björn; Fenske, Heinz-Dieter; Baum, Gerhard
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 1999
• Journal issue: 13
• Pages of publication: 1189 - 1190
• a: 24.82 ± 0.005 Å
• b: 20.98 ± 0.004 Å
• c: 26.87 ± 0.005 Å
• α: 90°
• β: 97.24 ± 0.03°
• γ: 90°
• Cell volume: 13880 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 8
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0888
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.1141
• Weighted residual factors for all reflections included in the refinement: 0.1301
• Goodness-of-fit parameter for all reflections included in the refinement: 0.903
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No