Information card for entry 7110802

Structure parameters

• Formula: C56 H60 Ir2 P2 Pd2 Se3
• Calculated formula: C56 H60 Ir2 P2 Pd2 Se3
• Title of publication: Syntheses of a dinuclear Ir complex containing bridging tetraselenide ligands [(C5Me5)Ir(μ-Se4)2Ir(C5Me5)] and its conversion into Ir2Pd2Se3 and Ir2Pd3Se5 clusters
• Authors of publication: Nagao, Shoken; Seino, Hidetake; Mizobe, Yasushi; Hidai, Masanobu
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 3
• Pages of publication: 207
• a: 18.884 ± 0.004 Å
• b: 11.066 ± 0.001 Å
• c: 26.778 ± 0.002 Å
• α: 90°
• β: 104.843 ± 0.008°
• γ: 90°
• Cell volume: 5409.1 ± 1.3 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.0424
• Weighted residual factors for all reflections included in the refinement: 0.0424
• Goodness-of-fit parameter for all reflections included in the refinement: 1.767
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No