Oxygen initiated unprecedented condensation of propargylamine into the 1,3-di(propargylimino)propylateanion coordinated to cobalt(iii)
Authors of publication
Sidorov, Aleksei A.; Ponina, Marina O.; Deomidov, Sergei M.; Novotortsev, Vladimir M.; Nefedov, Sergei E.; Eremenko, Igor L.; Moiseev, Ilya I.; Demonceau, Albert
Journal of publication
Chemical Communications
Year of publication
2000
Journal issue
15
Pages of publication
1383
a
14.83 ± 0.003 Å
b
15.354 ± 0.003 Å
c
15.282 ± 0.003 Å
α
90°
β
94.83 ± 0.03°
γ
90°
Cell volume
3467.4 ± 1.2 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0678
Residual factor for significantly intense reflections
0.0483
Weighted residual factors for all reflections
0.1344
Weighted residual factors for significantly intense reflections
0.1214
Goodness-of-fit parameter for all reflections
1.311
Goodness-of-fit parameter for significantly intense reflections
