Crystallography Open Database

Information card for entry 7111172

Preview

Coordinates	7111172.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H108 Ge2 P2
Calculated formula	C68 H108 Ge2 P2
Title of publication	Reaction of a diarylgermylene with a phosphaalkyne: formation of a germadiphosphacyclobutene with an exocyclic CGe double bond
Authors of publication	Meiners, Frank; Saak, Wolfgang; Weidenbruch, Manfred
Journal of publication	Chemical Communications
Year of publication	2001
Journal issue	2
Pages of publication	215
a	12.1315 ± 0.0006 Å
b	15.3937 ± 0.0008 Å
c	17.6016 ± 0.0007 Å
α	87.207 ± 0.005°
β	80.276 ± 0.005°
γ	87.046 ± 0.006°
Cell volume	3232.9 ± 0.3 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0901
Residual factor for significantly intense reflections	0.0455
Weighted residual factors for significantly intense reflections	0.0953
Weighted residual factors for all reflections included in the refinement	0.1064
Goodness-of-fit parameter for all reflections included in the refinement	0.862
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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