Syntheses and magnetic properties of hexanuclear [Cp2Mn3(L1)4]2 and octanuclear [Mn8(L2)12(μ4-O)2] (L1 = 2-HNC5H5N, L2 = 2-NH-3-Br-5-MeC5H3N, Cp = C5H5)
Authors of publication
Alvarez, Carmen Soria; Bond, Andrew D.; Cave, Dale; Mosquera, Marta E. G.; Harron, Eilís A.; Layfield, Richard A.; McPartlin, Mary; Rawson, Jeremy M.; Wood, Paul T.; Wright, Dominic S.
Journal of publication
Chemical Communications
Year of publication
2002
Journal issue
24
Pages of publication
2980 - 2981
a
31.3272 ± 0.0006 Å
b
33.194 ± 0.0007 Å
c
15.9032 ± 0.0004 Å
α
90°
β
90°
γ
90°
Cell volume
16537.3 ± 0.6 Å3
Cell temperature
180 ± 2 K
Ambient diffraction temperature
180 ± 2 K
Number of distinct elements
4
Space group number
43
Hermann-Mauguin space group symbol
F d d 2
Hall space group symbol
F 2 -2d
Residual factor for all reflections
0.0757
Residual factor for significantly intense reflections
0.0587
Weighted residual factors for significantly intense reflections
0.1648
Weighted residual factors for all reflections included in the refinement
0.1778
Goodness-of-fit parameter for all reflections included in the refinement
