Information card for entry 7111317

Structure parameters

• Chemical name: (S)-N-(3-buthoxycarbonyl-1-cyclohexylpropyl)-2,3-O- isopropylidene-5-deoxy-D-ribose-imine N-oxide
• Formula: C22 H39 N O6
• Calculated formula: C22 H39 N O6
• Title of publication: Radical addition of nitrones to acrylates mediated by SmI2: asymmetric synthesis of ?-amino acids employing carbohydrate-based chiral auxiliariesElectronic Supplementary Information (ESI) available: crystallographic data of 2b and 4a, experimental procedure and spectral data. See http://www.rsc.org/suppdata/cc/b4/b405141f/
• Authors of publication: Johannesen, Sine A.; Albu, Silvia; Hazell, Rita G.; Skrydstrup, Troels
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 17
• Pages of publication: 1962 - 1963
• a: 5.379 ± 0.001 Å
• b: 15.901 ± 0.003 Å
• c: 27.782 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2376.2 ± 0.8 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for all reflections included in the refinement: 0.054
• Goodness-of-fit parameter for all reflections included in the refinement: 1.247
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No