Information card for entry 7111425

Structure parameters

• Formula: C154 H220 N6 Ni32 O56 Pt24
• Calculated formula: C153.98 H219.96 N6 Ni32.04 O56 Pt24.002
• Title of publication: New high-nuclearity Ni?Pt carbonyl clusters: synthesis and X-ray structure of the ordered [HNi24Pt17(CO)46]5? and the substitutionally Ni/Pt disordered [Ni32Pt24(CO)56]6? cluster anions
• Authors of publication: Femoni, Cristina; Iapalucci, M. Carmela; Longoni, Giuliano; Svensson, Per H.
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 20
• Pages of publication: 2274 - 2275
• a: 29.477 ± 0.003 Å
• b: 29.477 ± 0.003 Å
• c: 22.178 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 16689 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.2363
• Residual factor for significantly intense reflections: 0.0655
• Weighted residual factors for significantly intense reflections: 0.1613
• Weighted residual factors for all reflections included in the refinement: 0.2012
• Goodness-of-fit parameter for all reflections included in the refinement: 0.81
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No