Information card for entry 7111542

Structure parameters

• Formula: C38 H62 B2 La N3 O2
• Calculated formula: C38 H62 B2 La N3 O2
• Title of publication: Unusual reactivity of lanthanide borohydride complexes leading to a borane complex
• Authors of publication: Meyer, Nils; Jenter, Jelena; Roesky, Peter W.; Eickerling, Georg; Scherer, Wolfgang
• Journal of publication: Chemical Communications
• Year of publication: 2009
• Journal issue: 31
• Pages of publication: 4693 - 4695
• a: 16.0927 ± 0.0008 Å
• b: 25.1371 ± 0.0017 Å
• c: 19.9083 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8053.4 ± 0.8 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0709
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0652
• Weighted residual factors for all reflections included in the refinement: 0.0723
• Goodness-of-fit parameter for all reflections included in the refinement: 0.864
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No