Information card for entry 7112005

Structure parameters

• Formula: C64 H118 N6 Na6 O82 P8 V10
• Calculated formula: C64 H76.0024 N6 Na6 O82 P8 V10
• Title of publication: Homologous size-extension of hybrid vanadate capsules - solid state structures, solution stability and surface deposition
• Authors of publication: Mariyatra B. Mahimaidoss; Sergey A. Krasnikov; Lukas Reck; Camelia I. Onet; John M. Breen; Nianyong Zhu; Bartosz Marzec; Igor V. Shvets; Wolfgang Schmitt
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 2265
• a: 12.144 ± 0.003 Å
• b: 12.144 ± 0.003 Å
• c: 49.317 ± 0.018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7273 ± 4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 128
• Hermann-Mauguin space group symbol: P 4/m n c
• Hall space group symbol: -P 4 2n
• Residual factor for all reflections: 0.2415
• Residual factor for significantly intense reflections: 0.1287
• Weighted residual factors for significantly intense reflections: 0.3085
• Weighted residual factors for all reflections included in the refinement: 0.3677
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No