Information card for entry 7112102

Structure parameters

• Formula: C93 H112 Cl4 Ge4 N8
• Calculated formula: C93 H112 Cl4 Ge4 N8
• Title of publication: Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond
• Authors of publication: Yan Li; Kartik Chandra Mondal; Peter Stollberg; Hongping Zhu; Herbert W. Roesky; Regine Herbst-Irmer; Dietmar Stalke; Heike Fliegl
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 3356
• a: 12.692 ± 0.002 Å
• b: 12.839 ± 0.002 Å
• c: 15.409 ± 0.003 Å
• α: 98.61 ± 0.02°
• β: 102.61 ± 0.02°
• γ: 113.07 ± 0.03°
• Cell volume: 2175.6 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0323
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0608
• Weighted residual factors for all reflections included in the refinement: 0.0639
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No