Information card for entry 7112984

Structure parameters

• Formula: C285 H345 Cl51 Co24 N36 O38 S24
• Calculated formula: C281.96 H333.96 Cl41.88 Co24 N36 O38 S24
• Title of publication: Making a [Co24] metallamacrocycle from the shuttlecock-like tetranuclear cobalt-calixarene building blocks.
• Authors of publication: Bi, Yanfeng; Xu, Guancheng; Liao, Wuping; Du, Shangchao; Wang, Xinwu; Deng, Ruiping; Zhang, Hongjie; Gao, Song
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 34
• Pages of publication: 6362 - 6364
• a: 28.1842 ± 0.0003 Å
• b: 28.1842 ± 0.0003 Å
• c: 46.3608 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 31892.8 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0833
• Residual factor for significantly intense reflections: 0.0656
• Weighted residual factors for significantly intense reflections: 0.2024
• Weighted residual factors for all reflections included in the refinement: 0.2142
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No