Crystallography Open Database

Information card for entry 7113286

Preview

Coordinates	7113286.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H29.5 Cl3 Mo N2.5 P2
Calculated formula	C37 H29.5 Cl3 Mo N2.5 P2
Title of publication	New coordination modes at molybdenum for 2-diphenylphosphinoaniline derived ligands
Authors of publication	Redshaw, Carl; Gibson, Vernon C.; Elsegood, Mark R. J.; Clegg, William
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2007
Journal issue	19
Pages of publication	1951 - 1953
a	12.3107 ± 0.0008 Å
b	13.0253 ± 0.0008 Å
c	21.6485 ± 0.0014 Å
α	90°
β	101.913 ± 0.002°
γ	90°
Cell volume	3396.6 ± 0.4 Å³
Cell temperature	160 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0282
Residual factor for significantly intense reflections	0.0247
Weighted residual factors for significantly intense reflections	0.0593
Weighted residual factors for all reflections included in the refinement	0.0614
Goodness-of-fit parameter for all reflections included in the refinement	1.097
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7101890
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7113286.html