Information card for entry 7113348

Structure parameters

• Common name: ((Mg((2,6-iPr2Ph)BIAN)(?-Me))2 (2) in paper)
• Formula: C81.5 H103.5 Mg2 N4
• Calculated formula: C74 H86 Mg2 N4
• Title of publication: Structural and EPR characterisation of single electron and alkyl transfer products from reaction of dimethyl magnesium with bulky alpha-diimine ligands.
• Authors of publication: Bailey, Philip J.; Coxall, Robert A.; Dick, Caroline M.; Fabre, Sylvie; Parsons, Simon; Yellowlees, Lesley J.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2005
• Journal issue: 36
• Pages of publication: 4563 - 4565
• a: 14.513 ± 0.007 Å
• b: 14.781 ± 0.009 Å
• c: 18.381 ± 0.009 Å
• α: 93.43 ± 0.04°
• β: 106.93 ± 0.03°
• γ: 100.09 ± 0.04°
• Cell volume: 3688 ± 4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1569
• Residual factor for significantly intense reflections: 0.097
• Weighted residual factors for significantly intense reflections: 0.2458
• Weighted residual factors for all reflections included in the refinement: 0.2867
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No