Crystallography Open Database

Information card for entry 7113467

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Coordinates	7113467.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H85 Br Mg O5 Pb4
Calculated formula	C74 H85 Br Mg O5 Pb4
Title of publication	Tris(triphenylplumbyl)plumbate: an anion with three stretched lead‒lead bonds
Authors of publication	Stabenow, Frank; Saak, Wolfang; Weidenbruch, Manfred
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2003
Journal issue	18
Pages of publication	2342 - 2343
a	15.699 ± 0.0004 Å
b	14.1672 ± 0.0005 Å
c	32.0448 ± 0.0007 Å
α	90°
β	95.009 ± 0.003°
γ	90°
Cell volume	7099.9 ± 0.3 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0855
Residual factor for significantly intense reflections	0.0373
Weighted residual factors for significantly intense reflections	0.0657
Weighted residual factors for all reflections included in the refinement	0.0748
Goodness-of-fit parameter for all reflections included in the refinement	0.835
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7104782
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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