Information card for entry 7113527

Structure parameters

• Formula: C27 H41 K N3 Sb
• Calculated formula: C27 H41 K N3 Sb
• SMILES: [Sb-]1c2c(C=C1c1cc(cc(c1)C)C)cc(cc2C)C.[K]12[N](C)(C)CC[N]1(C)CC[N]2(C)C
• Title of publication: Synthesis of a stibindolyl anion from trimesitylantimony and potassium
• Authors of publication: Breunig, Hans Joachim; Ghesner, Mihaiela Emilia; Lork, Enno
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 2
• Pages of publication: 274 - 275
• a: 23.681 ± 0.005 Å
• b: 9.641 ± 0.002 Å
• c: 13.243 ± 0.003 Å
• α: 90°
• β: 105.79 ± 0.03°
• γ: 90°
• Cell volume: 2909.4 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.0908
• Weighted residual factors for all reflections included in the refinement: 0.0965
• Goodness-of-fit parameter for all reflections included in the refinement: 0.923
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7103940
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No