Information card for entry 7113581

Structure parameters

• Formula: C128.5 H184 Al4 Li8 O7 P8
• Calculated formula: C128.5 H184 Al4 Li8 O7 P8
• Title of publication: Synthesis and structure of [{MeAl(μ-PMes)(PMes)}2Li4]2·7thf, containing a [MeAl(μ-PMes)(PMes)]24- tetraanion (Mes = 2,4,6-Me3C6H2)
• Authors of publication: García, Felipe; Haigh, Robert; McPartlin, Mary; Wright, Dominic S.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 16
• Pages of publication: 2052 - 2053
• a: 16.1493 ± 0.0003 Å
• b: 15.1393 ± 0.0002 Å
• c: 28.7338 ± 0.0005 Å
• α: 90°
• β: 90.063 ± 0.001°
• γ: 90°
• Cell volume: 7025.1 ± 0.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.1067
• Residual factor for significantly intense reflections: 0.0867
• Weighted residual factors for significantly intense reflections: 0.2223
• Weighted residual factors for all reflections included in the refinement: 0.2342
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7103846
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No