Information card for entry 7113634

Structure parameters

• Formula: C60 H94 P2 Sn2
• Calculated formula: C60 H94 P2 Sn2
• SMILES: [Sn]1(P[Sn](P1)(c1c(cc(cc1C(C)C)C(C)C)C(C)C)c1c(cc(cc1C(C)C)C(C)C)C(C)C)(c1c(cc(cc1C(C)C)C(C)C)C(C)C)c1c(cc(C(C)C)cc1C(C)C)C(C)C
• Title of publication: Synthesis of the first fluoro(phosphanyl)- and diphosphanyl-stannanes and surprising formation of [P(SnMe3)4]+SiF5-
• Authors of publication: Driess, Matthias; Merz, Klaus; Monsé, Christian
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 20
• Pages of publication: 2608 - 2609
• a: 10.538 ± 0.004 Å
• b: 16.379 ± 0.007 Å
• c: 17.76 ± 0.007 Å
• α: 103.08 ± 0.03°
• β: 91.27 ± 0.03°
• γ: 101.45 ± 0.03°
• Cell volume: 2919 ± 2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0789
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7104854
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No