Information card for entry 7113687

Structure parameters

• Formula: C162.67 H136 Co4 F36 N24 O15.11 P6
• Calculated formula: C162.664 H136 Co4 F36 N24 O15.112 P6
• Title of publication: A rigid cavity containing tetra-cobalt(III) [2 × 2] grid complex
• Authors of publication: Plante, Jeffrey P.; Jones, Paul D.; Powell, Douglas R.; Glass, Timothy E.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 3
• Pages of publication: 336 - 337
• a: 39.027 ± 0.004 Å
• b: 13.9229 ± 0.0013 Å
• c: 32.327 ± 0.003 Å
• α: 90°
• β: 113.855 ± 0.002°
• γ: 90°
• Cell volume: 16065 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1899
• Residual factor for significantly intense reflections: 0.0955
• Weighted residual factors for significantly intense reflections: 0.2503
• Weighted residual factors for all reflections included in the refinement: 0.3067
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7103942
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No