Information card for entry 7113944

Structure parameters

• Formula: C110 H104.5 Nb O3 P
• Calculated formula: C110 H104.5 Nb O3 P
• Title of publication: Binary role of an ylide in formation of a terminal methylidene complex of niobium
• Authors of publication: Keith Searles; Karlijn Keijzer; Chun-Hsing Chen; Mu-Hyun Baik; Daniel J. Mindiola
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 6267
• a: 14.8662 ± 0.0016 Å
• b: 39.237 ± 0.004 Å
• c: 15.5681 ± 0.0016 Å
• α: 90°
• β: 102.424 ± 0.005°
• γ: 90°
• Cell volume: 8868.3 ± 1.6 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0551
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for all reflections: 0.1235
• Weighted residual factors for significantly intense reflections: 0.119
• Weighted residual factors for all reflections included in the refinement: 0.1235
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9776
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No