Crystallography Open Database

Information card for entry 7114114

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Structure parameters

Formula	C18 H40 Cl Cu N7 Ni O8
Calculated formula	C18 H40 Cl Cu N7 Ni O8
Title of publication	Synthesis and characterization of [Cu(Me2oxpn)Ni(NO2)(tmen)](ClO4): a single ferrimagnetic dinuclear CuII–NiII complex acting as weak molecule-based magnet
Authors of publication	Tercero, Javier; Diaz, Carmen; Ribas, Joan; Mahía, José; Maestro, Miguel
Journal of publication	Chemical Communications
Year of publication	2002
Journal issue	4
Pages of publication	364
a	11.6156 ± 0.0001 Å
b	17.9957 ± 0.0003 Å
c	26.6134 ± 0.0001 Å
α	90°
β	90°
γ	90°
Cell volume	5563.02 ± 0.11 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	7
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0548
Residual factor for significantly intense reflections	0.0385
Weighted residual factors for significantly intense reflections	0.0858
Weighted residual factors for all reflections included in the refinement	0.0936
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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