Information card for entry 7114232

Structure parameters

• Formula: C203 H176 Cl12 N6 Ni7 O28
• Calculated formula: C203 H176 Cl12 N6 Ni7 O28
• Title of publication: Octanuclear cobalt and nickel cages featuring formate ligands
• Authors of publication: Cadiou, Cyril; Coxall, Robert A.; Graham, Alasdair; Harrison, Andrew; Helliwell, Madeleine; Parsons, Simon; Winpenny, Richard E. P.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 10
• Pages of publication: 1106
• a: 14.799 ± 0.009 Å
• b: 16.541 ± 0.009 Å
• c: 22.688 ± 0.012 Å
• α: 76.986 ± 0.015°
• β: 81.437 ± 0.018°
• γ: 78.429 ± 0.012°
• Cell volume: 5270 ± 5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.149
• Residual factor for significantly intense reflections: 0.1079
• Weighted residual factors for significantly intense reflections: 0.3072
• Weighted residual factors for all reflections included in the refinement: 0.322
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No