Information card for entry 7114257

Structure parameters

• Formula: C192 H168 N36 O36 Pd6
• Calculated formula: C365 H168 N24 O9 Pd6
• Title of publication: A molecular sphere of octahedral symmetryElectronic supplementary information (ESI) available: crystallography section; Figs. S1???S8: 1H NMR spectrum for 1. 1H, H???H COSY, NOESY, C???H COSY, 13C, DEPT NMR and CSI???MS spectra for 2. See http://www.rsc.org/suppdata/cc/b2/b206625b/
• Authors of publication: Chand, Dillip Kumar; Biradha, Kumar; Fujita, Makoto; Sakamoto, Shigeru; Yamaguchi, Kentaro
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 2486
• a: 34.312 ± 0.004 Å
• b: 34.312 ± 0.004 Å
• c: 29.063 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 34216 ± 7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 134
• Hermann-Mauguin space group symbol: P 42/n n m :2
• Hall space group symbol: -P 4ac 2bc
• Residual factor for all reflections: 0.2748
• Residual factor for significantly intense reflections: 0.1203
• Weighted residual factors for significantly intense reflections: 0.28
• Weighted residual factors for all reflections included in the refinement: 0.3134
• Goodness-of-fit parameter for all reflections included in the refinement: 1.397
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No