Crystallography Open Database

Information card for entry 7114260

Preview

Coordinates	7114260.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H59 F24 N12 O10 P4 Rh4
Calculated formula	C58 H50 F23 N12 O10 P4 Rh4
Title of publication	Coupling dirhodium units through terpyridine bridges: synthesis and structure of a novel molecular rectangle
Authors of publication	Bera, Jitendra K.; Campos-Fernández, Cristian Saul; Rodolphe, Clérac; Dunbar, Kim R.
Journal of publication	Chemical Communications
Year of publication	2002
Journal issue	21
Pages of publication	2536 - 2537
a	15.604 ± 0.005 Å
b	23.279 ± 0.005 Å
c	21.081 ± 0.005 Å
α	90°
β	110.158 ± 0.005°
γ	90°
Cell volume	7189 ± 3 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1084
Residual factor for significantly intense reflections	0.0755
Weighted residual factors for significantly intense reflections	0.1734
Weighted residual factors for all reflections included in the refinement	0.1906
Goodness-of-fit parameter for all reflections included in the refinement	1.098
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7114260.html