Information card for entry 7114281

Structure parameters

• Formula: C295 H312 Cl2 N24 Ni4 O33 Pd8
• Calculated formula: C295 H254 Cl2 N24 Ni4 O33 Pd8
• Title of publication: A modular approach to porphyrin oligomers using metal ions as connectorsElectronic supplementary information (ESI) available: preparation and spectroscopic data for compounds 4 and 6. Crystallographic data for the bis-palladium complex shown in Scheme 1. See http://www.rsc.org/suppdata/cc/b1/b109357f/
• Authors of publication: Richeter, S.; Jeandon, C.; Ruppert, R.; Callot, H. J.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 3
• Pages of publication: 266
• a: 15.8646 ± 0.0003 Å
• b: 21.1903 ± 0.0003 Å
• c: 23.5426 ± 0.0004 Å
• α: 73.875 ± 0.005°
• β: 77.767 ± 0.005°
• γ: 86.512 ± 0.005°
• Cell volume: 7430.4 ± 0.3 ų
• Cell temperature: 174 K
• Ambient diffraction temperature: 174 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.147
• Residual factor for significantly intense reflections: 0.066
• Weighted residual factors for all reflections: 0.61
• Weighted residual factors for all reflections included in the refinement: 0.1
• Goodness-of-fit parameter for all reflections: 15.812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.654
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No