Information card for entry 7114321

Structure parameters

• Formula: C52 H80 N4 Na O Yb
• Calculated formula: C52 H80 N4 Na O Yb
• Title of publication: Synthesis and structural characterization of imido‒lanthanide complexes with a metal‒nitrogen multiple bond
• Authors of publication: Chan, Hoi-Shan; Li, Hung-Wing; Xie, Zuowei
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 652
• a: 24.5164 ± 0.0011 Å
• b: 19.8148 ± 0.001 Å
• c: 24.5415 ± 0.0012 Å
• α: 90°
• β: 117.683 ± 0.001°
• γ: 90°
• Cell volume: 10557.3 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1206
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.0764
• Weighted residual factors for all reflections included in the refinement: 0.0927
• Goodness-of-fit parameter for all reflections included in the refinement: 0.809
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No