Information card for entry 7114339

Structure parameters

• Formula: C22 H10 Cl2 Eu F13 N2 O6
• Calculated formula: C21.5 H8 Cl Eu F13 N2 O6
• Title of publication: The first perfluoroacetylacetonate metal complexes: as unexpectedly robust as tricky to makeElectronic supplementary information (ESI) available: details of the preparation of the complexes, analytical, NMR spectroscopical, and crystallographic data. See: http://www.rsc.org/suppdata/cc/b1/b111249j/
• Authors of publication: Petrov, Viacheslav A.; Marshall, William J.; Grushin, Vladimir V.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 5
• Pages of publication: 520
• a: 11.7765 ± 0.001 Å
• b: 12.1403 ± 0.001 Å
• c: 12.8391 ± 0.001 Å
• α: 61.947 ± 0.01°
• β: 62.929 ± 0.01°
• γ: 64.341 ± 0.01°
• Cell volume: 1385.3 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0972
• Weighted residual factors for all reflections included in the refinement: 0.0989
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No