Information card for entry 7114370

Structure parameters

• Formula: C36 H31 F12 N6 O6.5 P2 Ru
• Calculated formula: C36 H30 F12 N6 O6.5 P2.001 Ru
• Title of publication: The isolation and secondary functionalisation of fac-tris-2,2′-bipyridine complexes of ruthenium(ii)Electronic supplementary information (ESI) availale: Table S1: Spectral data for 1‒5. Fig. S1: 1H NMR spectrum of 5. See http://www.rsc.org/suppdata/cc/b2/b202886g/
• Authors of publication: Fletcher, Nicholas C.; Nieuwenhuyzen, Mark; Prabarahan, Ravi; Wilson, Alison
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 11
• Pages of publication: 1188
• a: 11.9005 ± 0.0017 Å
• b: 20.52 ± 0.003 Å
• c: 16.71 ± 0.003 Å
• α: 90°
• β: 96.937 ± 0.002°
• γ: 90°
• Cell volume: 4050.7 ± 1.1 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1394
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1249
• Weighted residual factors for all reflections included in the refinement: 0.166
• Goodness-of-fit parameter for all reflections included in the refinement: 0.945
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No