Information card for entry 7114396

Structure parameters

• Chemical name: tetrahydrofurane-1,4,7,10-tetraoxacyclododecane- bis(trimethylsilylmethyl)lutetium(III)- trimethylsilylmethyltriphenylborate
• Formula: C42 H72 B Lu O5 Si3
• Calculated formula: C42 H72 B Lu O5 Si3
• Title of publication: The first structurally characterized cationic lanthanide‒alkyl complexesElectronic supplementary information (ESI) available: experimental and spectroscopic details. See http://www.rsc.org/suppdata/cc/b2/b201613n/
• Authors of publication: Arndt, Stefan; Spaniol, Thomas P.; Okuda, Jun
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 8
• Pages of publication: 896
• a: 11.014 ± 0.001 Å
• b: 12.633 ± 0.001 Å
• c: 17.433 ± 0.001 Å
• α: 93.706 ± 0.002°
• β: 94.301 ± 0.002°
• γ: 104.342 ± 0.002°
• Cell volume: 2334.7 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0216
• Residual factor for significantly intense reflections: 0.0198
• Weighted residual factors for significantly intense reflections: 0.0505
• Weighted residual factors for all reflections included in the refinement: 0.0511
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No