Information card for entry 7114464

Structure parameters

• Formula: C26 H43 N O5 P2 Si4 W
• Calculated formula: C26 H43 N O5 P2 Si4 W
• SMILES: [W]([P]1(P(C([Si](C)(C)C)[Si](C)(C)C)C(=N1)c1ccccc1)C([Si](C)(C)C)[Si](C)(C)C)(C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Synthesis of the first 2,3-dihydro-1,2,3-azadiphosphete complex
• Authors of publication: Ionescu, E.; Jones, P. G.; Streubel, R.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 19
• Pages of publication: 2204 - 2205
• a: 14.7253 ± 0.0008 Å
• b: 13.0428 ± 0.0008 Å
• c: 18.8621 ± 0.0012 Å
• α: 90°
• β: 97.072 ± 0.004°
• γ: 90°
• Cell volume: 3595.1 ± 0.4 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0476
• Residual factor for significantly intense reflections: 0.0217
• Weighted residual factors for significantly intense reflections: 0.04
• Weighted residual factors for all reflections included in the refinement: 0.0448
• Goodness-of-fit parameter for all reflections included in the refinement: 0.916
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No