Information card for entry 7114699

Structure parameters

• Formula: C97 H150 N4 Ni14.08 O31 Pt9.92
• Calculated formula: C97 H150 N4 Ni14.07 O31 Pt9.921
• Title of publication: New high-nuclearity Ni‒Pt carbonyl clusters: synthesis and X-ray structure of the ordered [Ni24Pt14(CO)44]4‒ and the substitutionally Ni/Pt disordered [Ni10(Ni6‒xPtx)Pt8(CO)30]4‒ (x = 1.92) tetraanions
• Authors of publication: Femoni, Cristina; Carmela Iapalucci, M.; Longoni, Giuliano; Svensson, Per H.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 18
• Pages of publication: 1776
• a: 26.7155 ± 0.0009 Å
• b: 15.2758 ± 0.0005 Å
• c: 31.9982 ± 0.0011 Å
• α: 90°
• β: 98.404 ± 0.001°
• γ: 90°
• Cell volume: 12918.3 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1257
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.0924
• Weighted residual factors for all reflections included in the refinement: 0.1162
• Goodness-of-fit parameter for all reflections included in the refinement: 0.888
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No