Information card for entry 7114722

Structure parameters

• Formula: C28 H35 N2 P Pd Si
• Calculated formula: C28 H35 N2 P Pd Si
• Title of publication: Preparation, structure and catalytic properties of a binuclear Pd(0) complex with bridging silylene ligands
• Authors of publication: Fürstner, Alois; Krause, Helga; Lehmann, Christian W.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 22
• Pages of publication: 2372
• a: 10.2277 ± 0.0002 Å
• b: 10.8525 ± 0.0002 Å
• c: 13.8201 ± 0.0002 Å
• α: 66.9°
• β: 73.51°
• γ: 89.89°
• Cell volume: 1342.49 ± 0.04 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0291
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.069
• Weighted residual factors for all reflections included in the refinement: 0.0711
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No