Information card for entry 7114872

Structure parameters

• Formula: C56 H56 Au2 F6 O8 P4 S2
• Calculated formula: C56 H48 Au2 F6 O8 P4 S2
• Title of publication: Observation of a P/M interconversion of a gold–phosphine helicate via   31P NMR
• Authors of publication: Schuh, Walter; Kopacka, Holger; Wurst, Klaus; Peringer, Paul
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 21
• Pages of publication: 2186
• a: 14.672 ± 0.002 Å
• b: 14.88 ± 0.001 Å
• c: 16.379 ± 0.002 Å
• α: 91.912 ± 0.006°
• β: 111.136 ± 0.005°
• γ: 115.533 ± 0.005°
• Cell volume: 2932.9 ± 0.6 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0844
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for all reflections: 0.1207
• Weighted residual factors for significantly intense reflections: 0.101
• Goodness-of-fit parameter for all reflections: 1.043
• Goodness-of-fit parameter for significantly intense reflections: 1.115
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No