Information card for entry 7114915

Structure parameters

• Chemical name: Bis[bis(diethylenetriamine)nickel(ii)]Bis[cyclo-octasulfido- tetraantimonate(iii)]
• Formula: C16 H52 N12 Ni2 S8 Sb4
• Calculated formula: C16 H52 N12 Ni2 S8 Sb4
• Title of publication: Solvothermal synthesis of [Ni(C4H13N3)2]2Sb4S8: the first compound with a cyclic [Sb4S8]4− anion
• Authors of publication: Bensch, Wolfgang; Näther, Christian; Stähler, Ralph
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 5
• Pages of publication: 477
• a: 9.0249 ± 0.0006 Å
• b: 12.7597 ± 0.001 Å
• c: 18.0367 ± 0.0013 Å
• α: 92.299 ± 0.009°
• β: 91.058 ± 0.008°
• γ: 105.735 ± 0.009°
• Cell volume: 1996.6 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0775
• Weighted residual factors for all reflections included in the refinement: 0.0814
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No