Information card for entry 7114946

Structure parameters

• Common name: {Cu6(tib)8(OH)4](OH)8.4CH3OH.22H2O
• Formula: C37 H54 Cu1.5 N12 O9.5
• Calculated formula: C37 H37 Cu1.5 N12 O9.5
• Title of publication: Assembly of a 3D nanoporous framework [Cu6(OH)4(tib)8]n8+ from Cu(ii) and the flexible tripodal ligand tib
• Authors of publication: Liu, Hong-Ke; Tan, Hai-Yan; Liao, Sen; Xiao, Wen; Zhang, Hua-Xin; Yu, Xiao-Lan; Kang, Bei-Sheng; Cai, Ji-Wen; Zhou, Zhong-Yuan; Chan, Albert S. C.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 11
• Pages of publication: 1008
• a: 13.662 ± 0.002 Å
• b: 23.197 ± 0.004 Å
• c: 18.914 ± 0.004 Å
• α: 90°
• β: 110.074 ± 0.003°
• γ: 90°
• Cell volume: 5630 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.167
• Residual factor for significantly intense reflections: 0.092
• Weighted residual factors for significantly intense reflections: 0.271
• Weighted residual factors for all reflections included in the refinement: 0.3207
• Goodness-of-fit parameter for all reflections included in the refinement: 0.961
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No