Information card for entry 7115042

Structure parameters

• Formula: C30 H60 B2 Li O3 P
• Calculated formula: C30 H60 B2 Li O3 P
• Title of publication: Formation of the monoanion [Ar*P(BH3)(µ-BH2)2H]‒ with a symmetrically bridging hydride from the attempted synthesis of the dianion [Ar*P(BH3)3]2‒
• Authors of publication: Rudzevich, Valentyn L.; Gornitzka, Heinz; Romanenko, Vadim D.; Bertrand, Guy
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 17
• Pages of publication: 1634
• a: 9.4853 ± 0.0005 Å
• b: 11.0044 ± 0.0005 Å
• c: 32.8968 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3433.8 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.1215
• Weighted residual factors for all reflections included in the refinement: 0.1299
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No