Information card for entry 7115051

Structure parameters

• Formula: C24 H14 Co N4 O8.5 V3
• Calculated formula: C24 H14 Co N4 O8.5 V3
• Title of publication: Dehydrogenative coupling of phenanthroline under hydrothermal conditions: crystal structure of a novel layered vanadate complex constructed of 4,8,10-net sheets: [(2,2′-biphen)Co]V3O8.5
• Authors of publication: Liu, Cai-Ming; Gao, Song; Kou, Hui-Zhong
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 17
• Pages of publication: 1670
• a: 19.66 ± 0.004 Å
• b: 18.43 ± 0.004 Å
• c: 13.64 ± 0.003 Å
• α: 90°
• β: 103.2 ± 0.03°
• γ: 90°
• Cell volume: 4811.7 ± 1.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0523
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.1046
• Weighted residual factors for all reflections included in the refinement: 0.1125
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No